Copper and Nickel Nanoparticles Prepared by Thermal Treatment of Their Respective Cations Confined in Nanopores through High-Pressure Synthesis
نویسندگان
چکیده
A new and simple method for preparing confined copper nickel nanoparticles by thermal treatment of their respective cations inside Mobil Composition Matter 41 (MCM–41) hydrophobic nanopores is presented here. Surface modified MCM–41 materials were impregnated using high-pressure with II (Cu II) or (Ni aqueous solutions. After pressure release washing, the remaining metal cations, exclusively within nanopores, heated, forming metallic nanoparticles. Reduction a redox reaction between organic surface proposed. Transmission electronic microscopy (TEM), selected area electron diffraction (SAED), nitrogen (N2) adsorption at −196 °C (77 K), Fourier transform infrared (FTIR) thermogravimetric (TGA) analyses evidenced identification (NPs).
منابع مشابه
Copper Oxide Nanoparticles Prepared by Solid State Thermal Decomposition: Synthesis and Characterization
In this paper, we have focused on the preparation and characterization of copper oxide nanoparticles by solid state thermal decomposition of copper(I) iodide in the presence of thiosemicarbazone ligands without the need for a catalyst, employing toxic solvent, template or surfactant and complicated equipment, which makes it efficient, one-step, simple and environment-friendly. CuO nanoparticles...
متن کاملNickel Oxide (NiO) nanoparticles prepared by solid-state thermal decomposition of Nickel (II) schiff base precursor
In this paper, plate-like NiO nanoparticles were prepared by one-pot solid-state thermal decomposition of nickel (II) Schiff base complex as new precursor. First, the nickel (II) Schiff base precursor was prepared by solid-state grinding using nickel (II) nitrate hexahydrate, Ni(NO3)2∙6H2O, and the Schiff base ligand N,N′-bis-(salicylidene) benzene-1,4-diamine) for 30 min without using any solv...
متن کاملSynthesis and characterization of Nickel (II) Chloride nanoparticles with the study of their thermal behavior
In this research nanoparticles of Nickel (II) Chloride were synthesized and characterized using fourier transform infrared (FT-IR) spectra. Nanoparticles of Nickel (II) Chloride were prepared by using of ball mill device. A ball mill is one kind of grinding machine, and it is a device in which media balls and solid materials (the materials to be ground) are placed in a container. In the researc...
متن کاملSynthesis and characterization of Copper and Copper Oxide nanoparticles by thermal decomposition method
A simple method has been employed to synthesize Copper and Copper oxide nanoparticles from Copper (II) succinate precursor by thermal decomposition method using oleylamine as a capping agent. The particles synthesized with oleylamine and triphenylphosphine were well dispersed nanoparticles obtained from X-ray Diffraction (XRD). The Synthesized copper nanoparticles were characterized by UV-Visib...
متن کاملSynthesis and characterization of Copper and Copper Oxide nanoparticles by thermal decomposition method
A simple method has been employed to synthesize Copper and Copper oxide nanoparticles from Copper (II) succinate precursor by thermal decomposition method using oleylamine as a capping agent. The particles synthesized with oleylamine and triphenylphosphine were well dispersed nanoparticles obtained from X-ray Diffraction (XRD). The Synthesized copper nanoparticles were characterized by UV-Visib...
متن کاملذخیره در منابع من
با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید
ژورنال
عنوان ژورنال: Applied nano
سال: 2021
ISSN: ['2673-3501']
DOI: https://doi.org/10.3390/applnano2030020